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Development of Sensing Material for Catalyst Combustion Type Methane Sensor

Author: YangYueHua
Tutor: ZhangTong
School: Jilin University
Course: Microelectronics and Solid State Electronics
Keywords: Contact combustion type gas sensor Template Methane Al2O3 Hydrothermal method
CLC: TP212.2
Type: Master's thesis
Year: 2010
Downloads: 85
Quote: 1
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Abstract


Catalytic combustion type sensors sensitive material prepared by several different methods , and its characterization and sensitivity characteristics test . Pd/Al2O3 catalyst material first prepared using traditional methods , Al2 (SO4) 3 and Na2CO3 as raw material , through precipitation method of γ-Al2O3 by vacuum distillation Pd supported on γ-Al2O3 . By examining the sintering temperature of the specific surface area of the carrier material and polymorphs , and ultimately chose the 750 ° C sintered materials . Hydrothermal ( solvothermal ) prepared Pd/Al2O3 catalyst material to Al (NO3) 3 and Pd (NO3) 2 as a raw material , the Pd/Al2O3 catalyst material was synthesized by hydrothermal reaction step , studies have shown that the type of solvent catalyst the characteristics of the material has a great influence . Finally template synthesis material of the SBA-15 , the use of a surfactant P123 ( polyoxyethylene - polyoxypropylene - polyoxyethylene) , and by the ion exchange method of Pd loaded on the SBA-15 . The catalyst prepared in a sensitive characteristic test , the first test of the loading amount of Pd on the device performance , the higher the amount of loading is possible to improve the long term stability of the device ; Hydrothermal Synthesis of a catalyst , using reductive than prepared in the strong solvent materials have a high sensitivity; using templates prepared SBA-15 material, due to large specific surface area , compared with the carrier prepared by conventional methods , with better sensitivity characteristics .

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CLC: > Industrial Technology > Automation technology,computer technology > Automation technology and equipment > Automation components,parts > Transmitter ( converter),the sensor > Chemical sensors
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