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Studies on the Quality Evaluation and Establishment of Quality Standard of Bulbus Fritillariae Thunbergh Produced in Zhejiang Province

Author: LiuHuiYing
Tutor: WangHePing
School: Heilongjiang University of Traditional Chinese Medicine
Course: Pharmacy
Keywords: Zhejiang Fritillaria Content determination HPLC-ELSD Quality standards
CLC: R282
Type: Master's thesis
Year: 2007
Downloads: 425
Quote: 1
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Abstract


Zhejiang Fritillaria Liliaceae Fritillaria thunbergii Fritillaria thunbergii Miq . Bulbs. Lung, the effect of the heat Sanjie . For wind-heat or phlegm cough, lung carbuncle spit pus M. scrofulaceum gallae , sore carbuncle swollen poison . This paper determines the optimum : Zhejiang Fritillaria alkaloids extracted 2 times amount of ammonia infiltration 15min 20 times amount of chloroform 80 ° C heating reflux extraction 4h . This method and Ningbo Xiangshan , Yinxian zhangcun , Jinhua Pan'an three producing areas , early April and late May the two harvest period and Wash break apart , dried , the Gefen dry and quicklime sucking 12 batches of three original processing method planted Zhejiang Fritillaria total alkaloid content determination , and further determination of the 12 batches of herbs medicinal components peimine the peiminine content , comprehensive assessment to determine the the best place of origin , the best harvest time , processing methods, namely the Yinxian zhangcun with Jinhua Pan'an collected in early April , directly wash break apart , dried Zhejiang Fritillaria quality . The further higher total alkaloid content of Yin the river , zhangcun , Jinhua three Origin harvest in early April , a total of 10 batches of Zhejiang Fritillaria system of quality standards Research , determination of the ash, moisture , extract indicators and measured by HPLC-ELSD method peimine the peiminine content , to determine the of Zhejiang geoherbs Zhejiang Fritillaria standard , in order to consolidate Zhejiang Province as Zhejiang Fritillaria Road area of real estate advantage.

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