Dissertation > Excellent graduate degree dissertation topics show

Research on the Performance and Interfacial Bonding of Nano-diamond/Ni Composite Coatings by Brush-Plating

Author: LiBianXiao
Tutor: LiYing
School: Henan University of Technology
Course: Materials Science
Keywords: nano-diamond composite coating interfacial bonding reinforcement mechanism
CLC: TB383
Type: Master's thesis
Year: 2011
Downloads: 85
Quote: 0
Read: Download Dissertation

Abstract


Ni-base plating coating and n-diamond/Ni composite coating are prepared respectivelyon Q235#steel matrix by using ultra-high energy mechanical and chemical techniques(HEMC).Again, the technical parameter are optimized by single factor and orthogonal designexperiments. The performance, the morphology and the composition of the interface areanalyzed. And the relationship between the nucleation and growth of nano-crystal and thecharacteristics of brush plating are introduced, the strengthening mechanism ofnano-diamond/Ni coating are also discussed.The results shows that: the dispersed evenly nano-diamond composite-coating areprepared by ultrasonic oscillation,mixing methods,also adding the op-10all together. Theoptimal parameters of the single factor and orthogonal experiments of the brush plating:voltage10V, bath temperature35~40℃, relatively speed11m/min, the content ofnano-diamond in plating5~30g/L, the coating thickness in control50μm around.The test results about frictional wear and hardness illustrated that the performance ofn-diamond/Ni coating is superior to that of rapid Ni-base coating such as higher hardness,higher wear-resistance, high-temperature properties. The wearing loss of the compositecoating is only1/3times than Ni-coating. When the nano-diamond density in the solution is30g/L, the microhardness of n-diamond/Ni composite coating has maximum value. And at200℃, the microhardness can reach687HV. During the coating tests of Bonding strength, nofalling off, cracking, peeling and so on, so the bonding strength is well.Through the analysis of the surface and interface,the cross-section organizations ofcoating has a "beam nodose organization" and "chain ring organization"; the hardness and thed-1/2essentially has a linear relationship, which fit the “Hall-Petch”. The deposition of nickelions is studied by cyclic voltammetry on nickel-plating bath. Then the mechanism ofinterfacial bonding of the coating is introduced and the interface structure, composition andconditions of combination are discussed by metallographic microscope, scanning electronmicroscope (SEM) energy dispersive spectrometry (EDS). Finally, the possibility of theformation of nano-crystalline are presented and the relationship between the nucleation andgrowth of nano-crystal and the characteristics of brush plating are analyzed; the strengtheningmechanism of nano-diamond/Ni coating are discussed, mainly involving fine-crystal, dispersion strengthening, dislocation strengthening.

Related Dissertations

  1. Preparation of the Composite Coatings on the Carbon Steel Surface and Their Anticorrosion Properties in Seawater,TG174.4
  2. The Study of Microstructure and Performance of La2 O3+CeO2-Ni-WC Composite Coating by Vacuum Fusion Sintering,TG174.44
  3. Preparation and Properties of Polyimide Nanocomposites,TB383.1
  4. Study on Repairing Material of Cement Concrete Pavement Which Based on Slag,U414
  5. Study on Process and Properties of Ni-P-Nano TiO2 Composite Coating on Magnesium Alloy,TG174.44
  6. The Research on Vacuum and Embankment Preloading Method Applied to the Treatment of Soft Soil Foundation,U416.1
  7. Study on the Construction Technology and Equipment of Cement Gravel Mixing Trenchless,U418.5
  8. Study on Soft Ground Treatment by Joint Methods of Vibration Crowded Gravel Pile and PHC Pile,U416.1
  9. Dynamic compaction and filling roadbed in Miscellaneous Engineering Mechanism,U416.1
  10. Study on the Technology of Ecological Protection in Broken Rockmass High Slope of Dianjiang to Linshui Freeway,U417.1
  11. Application Research of RENOLITH in Yunnan Pavement Engineering,U414
  12. Test Analysis and Numerical Simulation of Reinforced Red Sandstone Earth Retaining Wall by Geogrid,U417.11
  13. Experimental Study on Friction and Lubrication of Nano-two Phase Fluid,TB383.1
  14. Two-phase Flow Simulation of Ni-P-Diamond Electroless Composite Plating and Study on Its Plating Techniques,TQ153.1
  15. Detonation nanodiamonds stable dispersion in water research,TB383.1
  16. Quantum Properties of Single-Photon Emitter Coupled to Surface Plasmon,O431.2
  17. Microwave Assisted Deposition TiO_2 / nano-diamond and Electrochemical Performance,TB383.1
  18. Study on Surface Modifications and Electrochemical Properties of Nanodiamond,TB383.1
  19. The Research of Nano-diamond Coating FED Power Source and Driving Control System,TN873
  20. Investigation on the Preparation of Nano-diamond Field Emission Cathode by Electrophoretic Deposition,TN14
  21. Study of Nitrogen Effect on the Growth of Diamond Films,O484.1

CLC: > Industrial Technology > General industrial technology > Materials science and engineering > Special structural materials
© 2012 www.DissertationTopic.Net  Mobile