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Physical standard sample in the laboratory quality control and proficiency testing

Author: WuBin
Tutor: MaYiZhong；JiangYuan
School: Nanjing University of Technology and Engineering
Course: Industrial Engineering
Keywords: Honey Streptomycin Proficiency testing Physical standard sample Uncertainty Quality control chart Quality Control
CLC: S896.1
Type: Master's thesis
Year: 2011
Downloads: 34
Quote: 0
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Abstract


Laboratory quality control is the control measures taken for error control within the permissible limits of the analysis of the test results , which includes two parts laboratory quality control and laboratory quality control . Physical standards and proficiency testing is one of the most important elements of quality control and laboratory quality control laboratory . The paper kind standards for domestic research less honey , honey antibiotics testing data research and analysis of the laboratory and the EU Food and Feed Rapid Alert System (RASFF) 10 years honey antibiotics informed on the basis of screening out honey the detection rate of one of the antibiotics streptomycin physical standard sample preparation . Full analysis of the streptomycin standard solution preparation and stability , mechanical agitation physical standard sample preparation , column derivatization by high performance liquid chromatography - fluorescence detection method for setting using single factor analysis of variance (F test ) to test the kind of standard sample uniformity using physical standard samples t-test the stability tests of the past three months . Organizations nationwide proficiency testing ( Proficiency Test ) using Grubbs test , F test and Z-score test excluded outliers , analyze data and find outliers reason , kind of prepared standard sample last setting the uncertainty of the experimental results were evaluated. The setting is completed honey streptomycin physical standards established laboratory quality control charts , by drawing a good quality control chart for quality control laboratory in honey streptomycin daily detection analysis and guidance .

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CLC: > Agricultural Sciences > Livestock, animal medicine,hunting,silkworm,bee > Beekeeping,beneficial insects feeding > Bee products processing and utilization > Honey
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