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The Synthesis and Characterization of Metallophthalocyanine Initiator for Atom Transfer Radical Polymerization

Author: LiLiJun
Tutor: DuanQian
School: Changchun University of Science and Technology
Course: Applied Chemistry
Keywords: Phthalocyanine Phthalocyanine complexes Phthalonitrile Synthesis Characterization
CLC: TQ314.241
Type: Master's thesis
Year: 2010
Downloads: 52
Quote: 0
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Abstract


This thesis catechol , 2 - methoxy phenol as the raw material through the bromo- substituted and substituted cyanide were obtained 4,5 - docosyloxy phthalic dinitrile , 4 - [2 - ( 2 - bromo- ethoxy hydrogen pyran -4 ) ] -5 - methoxy -o- benzene dicarbonitrile eight substituted zinc phthalocyanine monomer was synthesized by the reaction in the 0 ° C an inert gas , to react with 2 - bromo - propionyl bromide for synthetic zinc phthalocyanine Jing initiator , and were characterized by IR and NMR spectroscopy .

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CLC: > Industrial Technology > Chemical Industry > Molecular compound Industries ( polymer industry ) > Raw materials and auxiliary materials > Synthetic polymer compound > Additives > Initiator
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