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Studies on Therapeutic Basis of Heigutengzhuifenghuoluojiaonang

Author: BanXiaoHong
Tutor: ZhangYuanHu;YangXiaoSheng
School: Guizhou University
Course: Medicinal Chemistry
Keywords: The black bone vine Herd active capsule Chemical Composition Qualitative and quantitative analysis
CLC: R286
Type: Master's thesis
Year: 2008
Downloads: 117
Quote: 0
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Abstract


Black bone the rattan Herd active capsules by the the Herd umbrella the ( from Lysimachia paridiformis Franch ) , Caulis (Sinomenium acutum Thunb.), The black bone vines (Periploca forrestiiSchltr.) Shamisen drug composition , the old blessing Pharmaceutical Group in Guizhou Province according to the theory of Miao Nationality Medicine , Miao medicine made ??in accordance with modern pharmaceutical technology . Clinical studies have shown that its acute and chronic rheumatoid arthritis , rheumatoid arthritis and other diseases have a significant effect, the clinical effective rate of 91.5% , and no reports of any side effects . This thesis is divided into three parts of its effective substances . The first part of the chemical composition and pharmacological effects of single herbs active capsules composed of a black bone vines Herd Summary , a total of 50 citations . The second part of the active the black bone vines Herd capsules experimental study of the chemical composition of natural product chemistry research tools and separation methods , combined with modern analytical techniques , of black bone vine Herd active capsules effective material composition system separation and structure identification. Separated from the compound 24 , identified 19 of them using modern spectroscopic techniques (NMR, EI-MS, FAB-MS , etc.) , of which seven alkaloids are the tip of tetrandrine sinomenine Anisakis tetrandrine Ivy ketone alkali , ivy given bat Gebo phenol alkali bat Radha . Lignin 5 were cloves resin diglucoside , THREO - 1- the C- syringyl -glycerol , ( - ) - the cloves resin phenol Cleomiscosin the C , Icariol A 2 < / sub > . Other compounds were ursolic acid , Yunnan Periplogenin A, syringaldehyde , syringic acid , catechol , periplocin , β- Valley sterol . Compound clear rotenone base for a new compound , and the rest of the compounds for the first time from the the black bone vines Herd active capsules isolated . 2 , by spectrophotometric determination of black bone vine Herd active capsules total alkaloid content . The sinomenine the standard curve Y = 6.7507x-0.0146 (r = 0.9995), showed that sinomenine in 0.04 ~ 0.20mg/mL range a good linear relationship between absorbance . Measured capsule total alkaloid content of 30.18%, RSD 2.31% . From mentioning the total alkaloid content of 42.65%, RSD 2.39% . Results and discussion of the third part of

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