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Studies on the Quality Standards and Extraction Technology of the Liriope Muscari in Fujian

Author: FuLiZuo
Tutor: SunWeiJiang
School: Fujian Agriculture and Forestry University
Course: Tea Science
Keywords: Fujian short Draba Liriope Quality standards Trace elements Polysaccharide Extract
CLC: R284
Type: Master's thesis
Year: 2008
Downloads: 275
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Abstract


The Fujian Liriope Liliaceae short Draba Liriope Liriope muscari (Decne.) Baily dry tuber (formerly known as Ophiopogon 1990), the authentic herbs in Fujian Province, is mainly produced in Quanzhou and Putian City, Fujian Province. Short Draba Liriope is contained in the received the Liriope under the Pharmacopoeia of the People's Republic of China (1995). Yin deficiency heat attending, Tianjin dry thirsty and dry expectoration thick, inverse gas or fever disability allowance, constipation embolism with YangYinShengJin lungs and pure heart, in addition to the effect of the dry An annoying. Short Draba Liriope flavor and meridian and function Indications Ophiopogon prescriptions medicine as Maidong equal, has become the mainstream of traditional Chinese medicine Ophiopogon commodity. This thesis research from four areas of Fujian short Draba Liriope quality results as follows: 1, Fujian short Draba Liriope origin of field data investigation, understanding Xianyou Fujian Ophiopogon records history Po Woo, Song Dynasty (AD 1254) 2012, the Modern began planting Liriope history more than 60 years, large output, which is now 50% of the normal dosage this short Draba Liriope Fujian Province geoherbs , and has become a the Ophiopogon Chinese herbs mainstream commodity. 2, the extraction process through short Draba Liriope polysaccharide single factor test and orthogonal test, the optimum extraction conditions: temperature of 90 ° C, the solid-liquid ratio of 1:30, a time of 3.5 h; extraction temperature on play a leading role in the extraction rate, solid-liquid ratio, extraction time was less affected. 3, take short Draba dried tuberous root of Liriope, paraffin sections, unarmed slice and powder slice, microscopic observation Liriope tissue morphology. In the Liriope powder film observed a large number of scattered or bunched needles into a piece of stone cells, as well as into beam or scattered in the wood fiber. Short Draba Liriope paraffin sections observed within the cortex outside the measured number of stone cells only one with the Hubei Maidong 1-2 rows of stone cells differentiated. The Liriope tuber cross-section of vascular large number, 16-22, This consistent description Pharmacopoeia and literature. 4, through the identification of Fujian short Draba Liriope saponins and sapogenin thin-layer chromatography and found to show the spots of the same color with the corresponding standard in sapogenin thin layer chromatography. 10 different regions of Fujian Liriope points on the same silica gel plates, thin-layer chromatogram of its ingredients are basically the same. In addition, the comparison of Ophiopogon japonicus Ophiopogon Hubei and Fujian short Draba Liriope, distinct thin layer chromatography (see Figure 4); using phenol - sulfuric acid method Fujian short Draba Liriope Liriope polysaccharide After the measurement, its maximum absorption peak at 489.9nm at an average recovery rate was 105.4% (n = 5, RSD = 2.04%), Fujian short Draba Liriope polysaccharide content in more than 31%, indicating that the method was simple fast, good reproducibility polysaccharide content determination method. Fujian of Liriope growth process in the alcohol-soluble extracts, water soluble, material, polysaccharides, trace elements and other indicators dynamic detection, based on their variation and combination of of Liriope production and origin climate factors, determined comprehensively 3 The late May Fujian Xianyou short Draba Liriope harvest period. Determination of useful inorganic elements in the Fujian short Draba Liriope obtained short Draba Liriope, Fe, Mg content is higher, most enrichment ability of zinc rich in these elements may be used in its treatment loss of appetite associated with suppression of the tumor as well as the prevention and treatment of cardiovascular disease. 6, on the basis of a comprehensive analysis of the test results, combined with literature data, to drafting of Fujian Liriope quality control standard. This paper argues that by determination of short Draba Liriope polysaccharide after acid hydrolysis monosaccharide content, then converted to the total amount of polysaccharide, as one of the quality standards of the Fujian short Draba Liriope, its content may not be less than 30% .

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