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Ma Xing Shi Gan Tang Different Combinations of calcium and inorganic ions

Author: TaoGuiBin
Tutor: GongJiYu
School: Changchun University of Traditional Chinese Medicine
Course: Pharmaceutical Analysis
Keywords: Ma Xing Shi Gan Tang Compatibility Inorganic ions Calcium-binding Free calcium Ion exchange resin Determination of content
CLC: R289
Type: Master's thesis
Year: 2010
Downloads: 63
Quote: 0
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Abstract


In this paper, Ma Xing Shi Gan Tang Different Combinations of inorganic ion content measurement and the presence of calcium in the form of research . Ma Xing Shi Gan Tang different compatibility calcium content by atomic absorption spectrophotometry , to study the impact of compatibility on the calcium content , more students of licorice Zhigancao calcium content . Method for determination of the regression equation was Abs = 0.00591C 0.00036, correlation coefficient ( r = 0.9998 ) , recovery was 101.4% . Ephedra and almonds increased amount of gypsum dissolution , licorice reduce Zhigancao more significant than raw licorice effect of reducing the amount of liquid in the gypsum dissolution of calcium were fried not significantly increase . Compatibility on Ma Xing Shi Gan Tang calcium content , this experiment for Maxingshigan soup Compatibility Law provides certain basis . L9 (34) orthogonal experiment to determine the 732 # type cation exchange resin separation of free calcium and calcium-binding experimental program . The analysis of variance showed to the concentration of the diluted sample as an indicator , the impact of combined calcium and ionized calcium separation process factors role in order to exchange column column height gt ; loading capacity gt ; fluid collection amount gt ; eluent volume , exchange column column , there are significant differences in the impact of the sample volume and the amount of fluid collection , with no significant difference in the amount of eluent , taking also into account economic factors , the best process: the sample volume for 100 ml of the ion exchange column column high 8 cm , the amount of 50 ml of eluent collected liquid amount 115 ml . Automatic SPE instrument separation of free calcium and calcium-binding compared with the ion exchange resin separation . Ma Xing Shi Gan Tang compatibility combined with calcium, separated by automatic solid-phase extraction instrument generally higher than ion exchange column to determine the content of the high content of calcium-binding . Determination of the results from a combination of calcium and free calcium content , automatic solid-phase extraction instrument its precision is much higher than the ion exchange resin , but also greatly reduces human error . In this paper, the experimental study of Ma Xing Shi Gan Tang compound active ingredient of the foundation.

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CLC: > Medicine, health > Chinese Medicine > Traditional Medical Formulae
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