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Porous molecular sieve material due to having an aperture adjustable, orderly and high adsorption better catalytic performance, good electromagnetic properties and is easy to cut, etc., in scientific research and technological applications aroused great interest. To further broaden its separation, catalysis, sensors and micro-devices and other fields of application, at present, at the micro (molecular level) control porous material composition, structure, and at the macro (large size) to control the appearance of the morphology of the porous material has become Research is an important direction of development. In this paper, we select a non-ionic surfactant as structure-directing agent, synthesis of different composition, structure, morphology and pore size of porous molecular sieve material. These studies will provide a porous material in the optical micro devices, bio-separation, and other fields to provide the necessary infrastructure, has a certain theoretical and practical significance. In this work, including the following: In the second chapter, a series of tri-block copolymer as a structure-directing agent, for the first time developed a non-aqueous solvent rapid evaporation induced self-assembly method of preparing large aperture, high degree of order Organic - Inorganic Hybrid Mesoporous Materials. Conventional \. Moreover, the method is to control the morphology of the mesoporous materials, convenient, simple methods. By solvent evaporation induced self-assembly techniques to three block copolymers such as P123 and F108 as structure-directing agent in the system, such as ethanol synthesis of a series of high order, large aperture (gt; 4 nm) with two-dimensional hexagonal structures and three-dimensional cubic structure, while the walls bismethylene containing mesoporous organic silica (PMO) materials. And by changing the experimental conditions, can effectively control their external morphology, having fibers, films, monolithic material such as morphology PMO. In addition, the use of solvent evaporation induced self-assembly of synthetic techniques to P123 triblock copolymer as a structure-directing agent, by solvent (hexane) heat treatment method, first prepare a high degree of order, large aperture (gt; 6 nm) and has a spiral channel structure (Ia3d) of PMO materials, breaking the ionic surfactant to prepare three-dimensional cubic structure PMO materials aperture limit. In synthesis, the solvent was changed P123 heat treatment after evaporation of the solvent in the assembly process, so that the formation of the accumulation of large curvature shape, the guide PMO synthetic material having a cube. As the material not only has a special composition and structure, but with a larger pore size (6.28 nm), the specific surface area (605 m ~ 2 / g) and pore volume (0.78 cm ~ 3 / g), in the preliminary tests found its drug molecule (norfloxacin) having good adsorption performance, so the load can be used as the main biological molecules. In the third chapter, the development of the traditional solvent evaporation induced self-assembly method for synthesizing organic alternative to using inorganic acid as an acid medium, prepared under anhydrous conditions similar mesoporous silica material. When tartaric acid as an acid medium, P123 as a structure-directing agent, for the first time in a non-aqueous system synthesized with the \The material has a \
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