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Synthesis, Characterization and Catalytic Proreties of Aluminosilicate with Hierarchical Porous Structure
Author: WangZhuZuo
Tutor: ZuoQiuBin
School: Jilin University
Course: Physical and chemical
Keywords: Zeolite Multi - level porous materials Mesoporous Carbon Template
CLC: TB383.4
Type: PhD thesis
Year: 2010
Downloads: 876
Quote: 0
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Abstract
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Microporous , mesoporous , macroporous materials from discovery to date in all aspects has been made a great deal of research progress , and is widely used in many areas of science and technology . However, in many applications the process , the researchers found that microporous , mesoporous and macroporous materials have their advantages and disadvantages , single use with a particular pore structure of the material is often not ideal , which is an urgent need for us to be able to come up with comprehensive variety of holes the structure of the material advantages of the new material , such as the preparation of new materials containing multi-level pore structure . This thesis is dedicated to the study of this new material contains a multi-level pore structure , elaborated a variety of multi-stage mesoporous materials synthesis conditions and methods , and the full characterization of their structural characteristics , physical and chemical properties and catalytic performance . The first chapter is the introduction , expounded the advantages and disadvantages of various porous materials , the history of the development and its application status . Which also introduced a multi-stage synthesis of porous materials principles , methods and their development status . Reagents and various test instrument model and test conditions ; Chapter hole wall crystallization method mesoporous material SBA -15 and JLU-1 hole wall crystallization synthesis of multi-level porous materials . In the fourth chapter , using the resin carbon as template synthesis of multi-level hole ZSM-5, another is water vapor crystallization of SiO2 - containing resin carbon to synthesize a multi-level hole ZSM - 5 . Chapter elaborate multi - level hole using porous polystyrene microspheres hard template synthesis of two different morphologies of Silicalite- 1 .
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